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2 article(s) from Kato, Kazuaki

Synthesis, structure, and mechanical properties of silica nanocomposite polyrotaxane gels

Kazuaki Kato,
Daisuke Matsui,
Koichi Mayumi and
Kohzo Ito

Beilstein J. Org. Chem. 2015, 11, 2194–2201, doi:10.3762/bjoc.11.238

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Figure 1: Nanocomposite polyrotaxane network formed by covalent bonds between cyclic components of polyrotaxa...

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Scheme 1: Synthesis of polyrotaxane with partially triethoxysilylated α-CDs (TES-PR) and crosslinking of the ...

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Figure 2: ¹H NMR spectra (400 MHz, DMSO-d₆, 343 K) of polyrotaxane and its derivatives with modified cyclic c...

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Figure 3: GPR traces of polyrotaxane and its derivatives; eluent: DMSO/LiBr (10 mM LiBr), detection: RI.

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Figure 4: Photograph of silica nanocomposite polyrotaxane gel.

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Figure 5: SAXS profiles of (a) silica nanocomposite polyrotaxane gels and (b) silica solutions with different...

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Figure 6: (a) Relaxation Young’s modulus with 5% strain and (b) frequency-dependence of dynamic storage and l...

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Figure 7: Repeated stress-strain curves for a silica nanocomposite polyrotaxane gel with 20% silica content.

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Full Research Paper

Published 16 Nov 2015

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Synthesis of graft polyrotaxane by simultaneous capping of backbone and grafting from rings of pseudo-polyrotaxane

Kazuaki Kato,
Katsunari Inoue,
Masabumi Kudo and
Kohzo Ito

Beilstein J. Org. Chem. 2014, 10, 2573–2579, doi:10.3762/bjoc.10.269

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Scheme 1: General synthetic scheme of graft polyrotaxane (GPR) consisting of 1) functionalization of polymer ...

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Scheme 2: Simplified synthetic scheme of graft polyrotaxane (GPR).

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Figure 1: Partial ¹H NMR (400 MHz, CDCl₃, 298 K) spectra of PEG-GA (above) and PGE-amine (below).

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Figure 2: SEC traces of GPR (run 1 in Table 1) and PEG derivatives. Eluents: DMSO/LiBr; detection: differential refr...

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Figure 3: ¹H NMR spectra (400 MHz, DMSO-d₆, 298 K) of GPRs: (a) run 1 and (b) run 2.

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Full Research Paper

Published 04 Nov 2014

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